How cold set

How cold set

Before set sample must be given certain prerequisites.To achieve correct set sample, you must first complete the following steps:

  • Clean the sample.With the sample之前,必须清洁试样以提高镶样介质与试样的粘附度。使用丙酮或酒精清洗。可能有必要在超声波浴中进行清洁。记得将试样擦干。清洗试样时,应当戴上手套或使用镊子。
  • Adjust the sample size,In accordance with the size of the sample cup

Cold inlaid type

There are two types of cold inlaid resin can be used epoxy resin and acrylic resin

Epoxy resin

Epoxy resin is suitable for the sample with all types of materials, particularly applicable to the vacuum impregnation.In all cold inlaid resin, epoxy resin shrinkage rate of the lowest.curing时间比较长,但是对大多数材料的粘附性能十分优异。在进行正确比例的混合后,它们通过化学反应进行聚合。硬化环氧树脂是硬质塑料,不受中等加热或化学品影响。Struers 的环氧树脂系统由两部分组成:树脂和固化剂/硬化剂。所有的环氧树脂都具有诸如低蒸气压、透明、高附着力、低粘度、无收缩等特性。作为化学计量树脂,固化剂比例是至关重要的。应该权衡这两个部分,以获得最佳的镶样结果。如果只能通过体积测量数量,可使用注射器来测量树脂和固化剂/硬化剂的数量

demo

curing

Depending on the amount of resin curing epoxy resin system.If resin quantity is little, this process may take longer, because there is easy to spread in addition to the advantageous conditions of excess heat generated by chemical reaction.But if the resin content, low thermal conductivity due to the reaction system, heat hoarding, and therefore can accelerate the cure process.Under certain conditions, the peak temperature can reach 150-200 ° C / 302-392 ° F.To avoid this situation, to achieve a more consistent set sample as a result, the drying box control in the process of curing temperature can be used.Resin hardened by polymerization.Aggregation is an exothermic reaction.The heat generated by the size depends on the type and number of sample with medium.Some kind of medium in the process of polymerization temperature significantly higher than 100 ℃.

Vacuum impregnation

Porous materials, such as ceramic or thermal spray coating) needs to be vacuum impregnation.Vacuum impregnation process in a vacuum chamber.Vacuum chamber pressure is about 0.1 to 0.15.Fill all the holes on the surface with resin.Resin can strengthen the fragile material.Can minimize the preparation of defects, such as pull out, crack or not open pore).Only epoxy resin can be used for vacuum impregnation, because they have low viscosity and low vapor pressure characteristics.Fluorescent dyes can be used mixed with epoxy resin, in order to find out everything under fluorescent light pore filling.Place the sample in sample cup, and put it in a vacuum chamber.Cover, a vacuum chamber.Lasts for a few minutes to process, to ensure that there is no air to stay in the small pore and fracture.Open the valve, make the inhalation of epoxy resin in vacuum chamber.When sample complete coverage in the sample with medium, close the valve and close the vacuum pump.The atmospheric pressure will epoxy resin pressure into pores and cracks.

Acrylic resin

Acrylic resin is easy to use, short curing time, has a very low degree of shrinkage and excellent with sample performance.They are very irregular shape of sample set new samples, can be used for routine or a single specimen.Acrylic resin offer attached and does not carry the two forms of mineral filler.If you need to color code, can be used to dye.in混合丙烯酸树脂时,建议向液体中添加粉末(硬化剂),这将生成最均匀的树脂混合物。

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Select set sample cup

Must consider the material and size cup.

size
Set the size of the sample cup should be enough to make sample and eventually set sample edge distance of 5 mm, as far as possible to reduce the risk of radial cracks.If the cup size relative to the sample size too much, can lead to excessive heat to damage the sample.If the ratio of resin to sample is bigger, shrinkage rate will also increase.

material
Epoxy resin curing will affect the silicon cup, shorten the life of sample set and transparency.in选择适用于丙烯酸树脂的杯材料时,存在不同的限制条件。

Set the sample process

Choose a set sample cup, put clean and dry the sample.Carefully measure the resin composition of the correct quantity (or weight by volume).Thoroughly mixing various ingredients, pour the mixture of resin on the sample, and make full set sample cup curing.To achieve high quality with sample, mixing and curing time is an important parameter.Should follow the instruction of the proposal.

Tolerance of common chemicals

All cold inlaid medium tolerance common etchant.But some cold inlaid medium can react with such as organic solvents such as acetone, alcohol

The fixed sample

Clamp (metal or plastic) ensures that keep it upright plate, foil and wire.Double adhesive foil can be used to make the irregular shape of sample keep it upright.Liquid binder may react with some types of cold inlaid medium.For sample is too small and not by the clamp (some electronic components, for example), use quick-drying glue them to the bottom of the mould, to make it keep in vertical position during embedding.

demo

Resin/selection guide

In order to achieve the desired effect, and can meet the requirement set sample, sample/medium is very important to select the correct resin.

This guide is intended to provide detailed information about the different cold Mosaic materials, tips and tricks.To the cold inlaid selection guidelines page

Guide to Cold Mounting materials

Troubleshooting - cold set with epoxy resin

The problem

Along the sample Side there bubbles
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why
High temperature curing process.

The solution:
Place sample on drying equipment or other well ventilated location, in order to reduce exposure temperature.Or, once in a layer of about 60 ml/sample set sample in resin (depending on the material), waiting for the first layer of hardening, and then set the next layer.
The reason:
Insufficient sample skim.

The solution:
The samples set sample before cleaning and degreasing.
The reason:
Mixing of the mixture is too severe.

The solution:
To avoid in the heart of the mixing process of air into the mixture.
The reason:
The surface tension.

The solution:
If possible, mobile samples after dumping of epoxy resin.
discoloration
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The reason:
High temperature curing process.

The solution:
Put the sample drying equipment, or other place with good ventilation.
The reason:
Resin volume compared with the sample size is too large.

The solution:
The sample using the appropriate set sample cup, or on drying equipment or other place with good ventilation, to eliminate the heat in the process of solidification.
The surface of the Sticky or rubber shaped
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The reason:
Curing temperature is too low.

The solution:
Insert the sample 30-50 ℃ / 86-122 ° F or in the oven for drying equipment after curing processing.
The reason:
Curing time is too short.

The solution:
Insert the sample 30-50 ℃ / 86-122 ° F or in the oven for drying equipment after curing processing.
The reason:
Too many curing agent relative to the resin.

The solution:
In the correct ratio of mixed resin and curing agent.
Shrink too much
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The reason:
High temperature curing process.

The solution:
Will set the sample cup in drying equipment, or other place with good ventilation.
The reason:
Insufficient sample skim.

The solution:
The samples set sample before cleaning and degreasing.
The reason:
Not fully mixed resin and curing agent.

The solution:
Fully stir the mixture of two to three minutes.
The reason:
Resin volume compared with the sample size is too large.

The solution:
The sample using the appropriate set sample cup, or on drying equipment or other place with good ventilation, to eliminate the heat in the process of solidification.
The reason:
Mixture volume is too large, or stirring after waiting a long time.

The solution:
Mixture volume reduction, and immediately fell on the sample after mixing.
in sample At the bottom of the suction/suction
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The reason:
High temperature curing process.

The solution:
Will set the sample cup in drying equipment, or other place with good ventilation.
The reason:
Resin volume compared with the sample size is too large.

The solution:
Using the appropriate set sample cup, or to set the sample cup in drying equipment or other place with good ventilation, to eliminate the heat in the process of solidification.Or, once in a layer of about 60 ml/sample set sample in resin (depending on the material), waiting for the first layer of hardening, and then set the next layer.
The bubble too much
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The reason:
High temperature curing process.

The solution:
Will set the sample cup in drying equipment, or other place with good ventilation.
The reason:
Mixing of the mixture is too severe.

The solution:
To avoid in the heart of the mixing process of air into the mixture.
The reason:
Resin volume compared with the sample size is too large.

The solution:
Using the appropriate set sample cup, or to set the sample cup in drying equipment or other place with good ventilation, to eliminate the heat in the process of solidification.
The reason:
Mixture volume is too large, or stirring after waiting a long time.

The solution:
Mixture volume reduction, and immediately fell on the sample after mixing.
Epoxy resin and sample No adhesion between
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The reason:
High temperature curing process.

The solution:
Will set the sample cup in drying equipment, or other place with good ventilation.
The reason:
Insufficient sample skim.

The solution:
The samples set sample before cleaning and degreasing.
The reason:
Resin volume compared with the sample size is too large.

The solution:
Using the appropriate set sample cup, or to set the sample cup in drying equipment or other place with good ventilation, to eliminate the heat in the process of solidification.
The reason:
Too many curing agent relative to the resin.

The solution:
In the correct ratio of mixed resin and curing agent.

Troubleshooting - cold set with acrylic acid

The problem

Along the sample profile of bubbles
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The reason:
Insufficient sample skim.

The solution:
Cleaning and degreasing sample before the sample set.
The reason:
The surface tension.

The solution:
After dumping resin mobile samples (if possible).
The reason:
Stir the mixture is too severe.

The solution:
Don't be in the process of mixing into the air.
The surface of the fat
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The reason:
Powder and liquid mixture of inadequate.

The solution:
Whisk together at least 30 seconds.
The reason:
Too much liquid relative to powder.

The solution:
In the correct ratio of mixed liquid and powder.
The bubble too much
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The reason:
Stir the mixture is too severe.

The solution:
Don't be in the process of mixing into the air.
No adhesion between resin and samples
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The reason:
Insufficient sample skim.

The solution:
Cleaning and degreasing sample before the sample set.
Sample with a rubber surface vein after cooling
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The reason:
Too much liquid relative to powder.

The solution:
In the correct ratio of mixed liquid and powder.
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